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Diffractometer

The diffractometer was designed such that a sphere of 65 mm radius around its center is free of mechanical components to avoid collisions with the detector system. It resembles a conventional 4-circle diffractometer with 0° < χ < 90° and can thus be used for the investigation of single crystallites and for texture analysis.↵

It can be applied to study lattice spacing and orientation as function of position in the specimen in order to reveal the influence of the surrounding (strain gradients, grain-grain interactions, etc.) and the impact of processing parameters (crystallization, thermal and mechanical treatment, etc.). The phi-circle of the instrument is equipped with an x,y (300 mm) and z (20 mm) translation allowing the investigation of large workpieces.↵

4-Circle Diffractometer

-90° < 2-θ < 150°
0° < Ω < 150°
0° < &chi < 90°
-180° < Φ < 180°

with xyz-Table

-80 mm < x,y < 120 mm
-10 mm < z < 10 mm

CCD-Detector

1000 x 1018 pixel of 12 µm x 12 µm

with Microchannel plate

thickness 4 mm
channel diameter 10 µm
center to center distance between channels 12.5 µm
diameter of active area 19 mm

NaJ-Detector with Soller slits

acceptance 0.15°


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